{"id":501,"date":"2021-09-14T07:31:11","date_gmt":"2021-09-14T07:31:11","guid":{"rendered":"https:\/\/foodsafety.upb.ro\/?page_id=501"},"modified":"2021-11-29T09:02:25","modified_gmt":"2021-11-29T09:02:25","slug":"laboratorul-de-analiza-termica-complexa","status":"publish","type":"page","link":"https:\/\/foodsafety.upb.ro\/en\/laboratorul-de-analiza-termica-complexa\/","title":{"rendered":"Complex thermal analysis laboratory"},"content":{"rendered":"\t\t<div data-elementor-type=\"wp-page\" data-elementor-id=\"501\" class=\"elementor elementor-501\" data-elementor-post-type=\"page\">\n\t\t\t\t\t\t<section class=\"elementor-section elementor-top-section elementor-element elementor-element-0d327d8 elementor-section-boxed elementor-section-height-default elementor-section-height-default\" data-id=\"0d327d8\" data-element_type=\"section\" data-e-type=\"section\" data-settings=\"{&quot;background_background&quot;:&quot;classic&quot;}\">\n\t\t\t\t\t\t\t<div class=\"elementor-background-overlay\"><\/div>\n\t\t\t\t\t\t\t<div class=\"elementor-container elementor-column-gap-default\">\n\t\t\t\t\t<div class=\"elementor-column elementor-col-100 elementor-top-column elementor-element elementor-element-29fe375\" data-id=\"29fe375\" data-element_type=\"column\" data-e-type=\"column\">\n\t\t\t<div class=\"elementor-widget-wrap elementor-element-populated\">\n\t\t\t\t\t\t<div class=\"elementor-element elementor-element-c812ebd elementor-widget elementor-widget-heading\" data-id=\"c812ebd\" data-element_type=\"widget\" data-e-type=\"widget\" data-widget_type=\"heading.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t<h2 class=\"elementor-heading-title elementor-size-default\">Laboratorul de analiz\u0103 termic\u0103 complex\u0103<\/h2>\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t<section class=\"elementor-section elementor-top-section elementor-element elementor-element-48de92e elementor-section-full_width elementor-section-height-default elementor-section-height-default\" data-id=\"48de92e\" data-element_type=\"section\" data-e-type=\"section\" data-settings=\"{&quot;sticky&quot;:&quot;top&quot;,&quot;sticky_on&quot;:[&quot;desktop&quot;,&quot;tablet&quot;],&quot;sticky_offset&quot;:0,&quot;sticky_effects_offset&quot;:0,&quot;sticky_anchor_link_offset&quot;:0}\">\n\t\t\t\t\t\t\t<div class=\"elementor-background-overlay\"><\/div>\n\t\t\t\t\t\t\t<div class=\"elementor-container elementor-column-gap-default\">\n\t\t\t\t\t<div class=\"elementor-column elementor-col-100 elementor-top-column elementor-element elementor-element-636cc7b\" data-id=\"636cc7b\" data-element_type=\"column\" data-e-type=\"column\">\n\t\t\t<div class=\"elementor-widget-wrap elementor-element-populated\">\n\t\t\t\t\t\t<section class=\"elementor-section elementor-inner-section elementor-element elementor-element-f826dfa elementor-section-boxed elementor-section-height-default elementor-section-height-default\" data-id=\"f826dfa\" data-element_type=\"section\" data-e-type=\"section\">\n\t\t\t\t\t\t<div class=\"elementor-container elementor-column-gap-default\">\n\t\t\t\t\t<div class=\"elementor-column elementor-col-50 elementor-inner-column elementor-element elementor-element-d6711e9\" data-id=\"d6711e9\" data-element_type=\"column\" data-e-type=\"column\">\n\t\t\t<div class=\"elementor-widget-wrap elementor-element-populated\">\n\t\t\t\t\t\t<div class=\"elementor-element elementor-element-a1cf291 elementor-align-justify elementor-widget elementor-widget-button\" data-id=\"a1cf291\" data-element_type=\"widget\" data-e-type=\"widget\" data-widget_type=\"button.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t\t\t<div class=\"elementor-button-wrapper\">\n\t\t\t\t\t<a class=\"elementor-button elementor-button-link elementor-size-sm elementor-animation-float\" href=\"#aparatdeanaliza\">\n\t\t\t\t\t\t<span class=\"elementor-button-content-wrapper\">\n\t\t\t\t\t\t\t\t\t<span class=\"elementor-button-text\">Aparat de analiz\u0103 complex\u0103 (ATD-DSC-TG-FTIR-MS)<\/span>\n\t\t\t\t\t<\/span>\n\t\t\t\t\t<\/a>\n\t\t\t\t<\/div>\n\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t<div class=\"elementor-column elementor-col-50 elementor-inner-column elementor-element elementor-element-8d6881f\" data-id=\"8d6881f\" data-element_type=\"column\" data-e-type=\"column\">\n\t\t\t<div class=\"elementor-widget-wrap elementor-element-populated\">\n\t\t\t\t\t\t<div class=\"elementor-element elementor-element-6003fa9 elementor-align-justify elementor-widget elementor-widget-button\" data-id=\"6003fa9\" data-element_type=\"widget\" data-e-type=\"widget\" data-widget_type=\"button.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t\t\t<div class=\"elementor-button-wrapper\">\n\t\t\t\t\t<a class=\"elementor-button elementor-button-link elementor-size-sm elementor-animation-float\" href=\"#echipamentdeanaliza\">\n\t\t\t\t\t\t<span class=\"elementor-button-content-wrapper\">\n\t\t\t\t\t\t\t\t\t<span class=\"elementor-button-text\">Echipament de analiz\u0103 elemental\u0103 CHNOS<\/span>\n\t\t\t\t\t<\/span>\n\t\t\t\t\t<\/a>\n\t\t\t\t<\/div>\n\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t<section class=\"elementor-section elementor-top-section elementor-element elementor-element-e99e2b7 elementor-section-boxed elementor-section-height-default elementor-section-height-default\" data-id=\"e99e2b7\" data-element_type=\"section\" data-e-type=\"section\">\n\t\t\t\t\t\t\t<div class=\"elementor-background-overlay\"><\/div>\n\t\t\t\t\t\t\t<div class=\"elementor-container elementor-column-gap-default\">\n\t\t\t\t\t<div class=\"elementor-column elementor-col-100 elementor-top-column elementor-element elementor-element-e58d9bd\" data-id=\"e58d9bd\" data-element_type=\"column\" data-e-type=\"column\">\n\t\t\t<div class=\"elementor-widget-wrap elementor-element-populated\">\n\t\t\t\t\t\t<div class=\"elementor-element elementor-element-4a588b4 elementor-widget elementor-widget-menu-anchor\" data-id=\"4a588b4\" data-element_type=\"widget\" data-e-type=\"widget\" data-widget_type=\"menu-anchor.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t<div class=\"elementor-menu-anchor\" id=\"aparatdeanaliza\"><\/div>\n\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<div class=\"elementor-element elementor-element-1e64a62 elementor-widget elementor-widget-heading\" data-id=\"1e64a62\" data-element_type=\"widget\" data-e-type=\"widget\" data-widget_type=\"heading.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t<h2 class=\"elementor-heading-title elementor-size-default\">Aparat de analiz\u0103 complex\u0103 (ATD-DSC-TG-FTIR-MS)\n<\/h2>\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<div class=\"elementor-element elementor-element-8d4b22e elementor-widget elementor-widget-spacer\" data-id=\"8d4b22e\" data-element_type=\"widget\" data-e-type=\"widget\" data-widget_type=\"spacer.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t<div class=\"elementor-spacer\">\n\t\t\t<div class=\"elementor-spacer-inner\"><\/div>\n\t\t<\/div>\n\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<section class=\"elementor-section elementor-inner-section elementor-element elementor-element-8b78c43 elementor-section-boxed elementor-section-height-default elementor-section-height-default\" data-id=\"8b78c43\" data-element_type=\"section\" data-e-type=\"section\">\n\t\t\t\t\t\t<div class=\"elementor-container elementor-column-gap-no\">\n\t\t\t\t\t<div class=\"elementor-column elementor-col-50 elementor-inner-column elementor-element elementor-element-b9fdaf7\" data-id=\"b9fdaf7\" data-element_type=\"column\" data-e-type=\"column\">\n\t\t\t<div class=\"elementor-widget-wrap elementor-element-populated\">\n\t\t\t\t\t\t<div class=\"elementor-element elementor-element-406c4ce elementor-widget elementor-widget-text-editor\" data-id=\"406c4ce\" data-element_type=\"widget\" data-e-type=\"widget\" data-widget_type=\"text-editor.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t\t\t<p><span style=\"font-weight: 400;\">Sistemul de analiz\u0103 termic\u0103 complex\u0103 format dintr-o termobalan\u0163\u0103 STA 449 C F3 de la Netzsch, care poate analiza pierderile de mas\u0103 \u00een intervalul -100 \u2013 1000<\/span><span style=\"font-weight: 400;\">o<\/span><span style=\"font-weight: 400;\">C (prin r\u0103cire cu azot lichid). Viteza de \u00eenc\u0103lzire a probei poate fi variat\u0103 \u00een intervalul 0.1-100 K\/min. Analizele se pot efectua \u00een atmosfer\u0103 inert\u0103 sau oxidant\u0103 (aer sintetic). Pot fi analizate probe solide sau lichide, cu masa cuprins\u0103 \u00eentre 10-50 mg. Se determin\u0103 pierderea \/ cre\u015fterea masei, efectele termice care \u00eenso\u0163esc reac\u0163iile chimice (descompunere, oxidare etc.) sau procesele fizice (topire, fierbere, solidificare, alte tranzi\u0163ii de faz\u0103).<\/span><\/p><p><span style=\"font-weight: 400;\">Gazele eliberate \u00een cursul analizei termice pot fi la r\u00e2ndul lor analizate prin cuplajul cu spectrometrul FTIR Tensor 27 de la Bruker \u015fi cu sistemul GC-MS de la JAS.<\/span><\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<div class=\"elementor-element elementor-element-8746479 elementor-widget elementor-widget-text-editor\" data-id=\"8746479\" data-element_type=\"widget\" data-e-type=\"widget\" data-widget_type=\"text-editor.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t\t\t<p><span style=\"font-weight: 400;\">Analiz\u0103 termic\u0103 pentru dou\u0103 probe de magnetit\u0103. O prob\u0103 este simpl\u0103 \u015fi o prob\u0103 este \u00eencapsulat\u0103 \u00een silice. Acoperirea cu silice protejeaz\u0103 magnetita de reac\u021biile de oxidare.<\/span><\/p><p><span style=\"font-weight: 400;\">Diagrama 3D ob\u021binut\u0103 din \u00eensumarea spectrelor FTIR ale gazelor eliminate func\u021bie de temperatura cuptorului. Se v\u0103d benzile caracteristice compu\u0219ilor organici la temperatur\u0103 joas\u0103 (p\u00e2n\u0103 \u00een 200<\/span><span style=\"font-weight: 400;\">o<\/span><span style=\"font-weight: 400;\">C) \u015fi apoi prezen\u021ba CO<\/span><span style=\"font-weight: 400;\">2<\/span><span style=\"font-weight: 400;\"> ob\u021binut din oxidarea compu\u0219ilor organici.<\/span><\/p><p><span style=\"font-weight: 400;\">Proiec\u0163ia 2D a spectrelor FTIR indic\u0103 cum se elimin\u0103 \u00een func\u0163ie de temperatur\u0103 anumite gaze. Se pot identifica procesele \u00een care au loc descompuneri, oxidari \u015fi c\u00e2nd CO \u00eenso\u0163e\u015fte CO<\/span><span style=\"font-weight: 400;\">2<\/span><span style=\"font-weight: 400;\">.\u00a0<\/span><\/p><p><span style=\"font-weight: 400;\">Gazele eliminate pot fi analizate prin FTIR sau GC-MS \u015fi se poate construi un profil al gener\u0103rii speciilor de interes (arderea spumei poliuretanice genereaza gaze toxice CO \u015fi HCN \u2013 cazul Colectiv).\u00a0<\/span><\/p><p><span style=\"font-weight: 400;\">\u00a0<\/span><\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t<div class=\"elementor-column elementor-col-50 elementor-inner-column elementor-element elementor-element-ea74f22\" data-id=\"ea74f22\" data-element_type=\"column\" data-e-type=\"column\" data-settings=\"{&quot;background_background&quot;:&quot;classic&quot;}\">\n\t\t\t<div class=\"elementor-widget-wrap elementor-element-populated\">\n\t\t\t\t\t\t<div class=\"elementor-element elementor-element-3dab5b2 elementor-widget elementor-widget-spacer\" data-id=\"3dab5b2\" data-element_type=\"widget\" data-e-type=\"widget\" data-widget_type=\"spacer.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t<div class=\"elementor-spacer\">\n\t\t\t<div class=\"elementor-spacer-inner\"><\/div>\n\t\t<\/div>\n\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t<div class=\"elementor-element elementor-element-282b8c7 elementor-widget elementor-widget-gallery\" data-id=\"282b8c7\" data-element_type=\"widget\" data-e-type=\"widget\" data-settings=\"{&quot;columns_mobile&quot;:2,&quot;lazyload&quot;:&quot;yes&quot;,&quot;gallery_layout&quot;:&quot;grid&quot;,&quot;columns&quot;:4,&quot;columns_tablet&quot;:2,&quot;gap&quot;:{&quot;unit&quot;:&quot;px&quot;,&quot;size&quot;:10,&quot;sizes&quot;:[]},&quot;gap_tablet&quot;:{&quot;unit&quot;:&quot;px&quot;,&quot;size&quot;:10,&quot;sizes&quot;:[]},&quot;gap_mobile&quot;:{&quot;unit&quot;:&quot;px&quot;,&quot;size&quot;:10,&quot;sizes&quot;:[]},&quot;link_to&quot;:&quot;file&quot;,&quot;aspect_ratio&quot;:&quot;3:2&quot;,&quot;overlay_background&quot;:&quot;yes&quot;,&quot;content_hover_animation&quot;:&quot;fade-in&quot;}\" data-widget_type=\"gallery.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t<div class=\"elementor-gallery__container\">\n\t\t\t\t\t\t\t<a class=\"e-gallery-item elementor-gallery-item elementor-animated-content\" href=\"https:\/\/foodsafety.upb.ro\/wp-content\/uploads\/2021\/10\/analiza-termica2.png\" data-elementor-open-lightbox=\"yes\" data-elementor-lightbox-slideshow=\"282b8c7\" data-elementor-lightbox-title=\"analiza termica2\" data-e-action-hash=\"#elementor-action%3Aaction%3Dlightbox%26settings%3DeyJpZCI6MTM4MywidXJsIjoiaHR0cHM6XC9cL2Zvb2RzYWZldHkudXBiLnJvXC93cC1jb250ZW50XC91cGxvYWRzXC8yMDIxXC8xMFwvYW5hbGl6YS10ZXJtaWNhMi5wbmciLCJzbGlkZXNob3ciOiIyODJiOGM3In0%3D\">\n\t\t\t\t\t<div class=\"e-gallery-image elementor-gallery-item__image\" data-thumbnail=\"https:\/\/foodsafety.upb.ro\/wp-content\/uploads\/2021\/10\/analiza-termica2.png\" data-width=\"624\" data-height=\"266\" aria-label=\"\" role=\"img\" ><\/div>\n\t\t\t\t\t\t\t\t\t\t\t<div class=\"elementor-gallery-item__overlay\"><\/div>\n\t\t\t\t\t\t\t\t\t\t\t\t\t\t<\/a>\n\t\t\t\t\t\t\t<a class=\"e-gallery-item elementor-gallery-item elementor-animated-content\" href=\"https:\/\/foodsafety.upb.ro\/wp-content\/uploads\/2021\/10\/analiza-termica-3.png\" data-elementor-open-lightbox=\"yes\" data-elementor-lightbox-slideshow=\"282b8c7\" data-elementor-lightbox-title=\"analiza termica 3\" data-e-action-hash=\"#elementor-action%3Aaction%3Dlightbox%26settings%3DeyJpZCI6MTM4NCwidXJsIjoiaHR0cHM6XC9cL2Zvb2RzYWZldHkudXBiLnJvXC93cC1jb250ZW50XC91cGxvYWRzXC8yMDIxXC8xMFwvYW5hbGl6YS10ZXJtaWNhLTMucG5nIiwic2xpZGVzaG93IjoiMjgyYjhjNyJ9\">\n\t\t\t\t\t<div class=\"e-gallery-image elementor-gallery-item__image\" data-thumbnail=\"https:\/\/foodsafety.upb.ro\/wp-content\/uploads\/2021\/10\/analiza-termica-3.png\" data-width=\"643\" data-height=\"552\" aria-label=\"\" role=\"img\" ><\/div>\n\t\t\t\t\t\t\t\t\t\t\t<div class=\"elementor-gallery-item__overlay\"><\/div>\n\t\t\t\t\t\t\t\t\t\t\t\t\t\t<\/a>\n\t\t\t\t\t\t\t<a class=\"e-gallery-item elementor-gallery-item elementor-animated-content\" href=\"https:\/\/foodsafety.upb.ro\/wp-content\/uploads\/2021\/10\/analiza-termica-4.png\" data-elementor-open-lightbox=\"yes\" data-elementor-lightbox-slideshow=\"282b8c7\" data-elementor-lightbox-title=\"analiza termica 4\" data-e-action-hash=\"#elementor-action%3Aaction%3Dlightbox%26settings%3DeyJpZCI6MTM4NSwidXJsIjoiaHR0cHM6XC9cL2Zvb2RzYWZldHkudXBiLnJvXC93cC1jb250ZW50XC91cGxvYWRzXC8yMDIxXC8xMFwvYW5hbGl6YS10ZXJtaWNhLTQucG5nIiwic2xpZGVzaG93IjoiMjgyYjhjNyJ9\">\n\t\t\t\t\t<div class=\"e-gallery-image elementor-gallery-item__image\" data-thumbnail=\"https:\/\/foodsafety.upb.ro\/wp-content\/uploads\/2021\/10\/analiza-termica-4.png\" data-width=\"643\" data-height=\"419\" aria-label=\"\" role=\"img\" ><\/div>\n\t\t\t\t\t\t\t\t\t\t\t<div class=\"elementor-gallery-item__overlay\"><\/div>\n\t\t\t\t\t\t\t\t\t\t\t\t\t\t<\/a>\n\t\t\t\t\t\t\t<a class=\"e-gallery-item elementor-gallery-item elementor-animated-content\" href=\"https:\/\/foodsafety.upb.ro\/wp-content\/uploads\/2021\/10\/analiza-termica-5.png\" data-elementor-open-lightbox=\"yes\" data-elementor-lightbox-slideshow=\"282b8c7\" data-elementor-lightbox-title=\"analiza termica 5\" data-e-action-hash=\"#elementor-action%3Aaction%3Dlightbox%26settings%3DeyJpZCI6MTM4NiwidXJsIjoiaHR0cHM6XC9cL2Zvb2RzYWZldHkudXBiLnJvXC93cC1jb250ZW50XC91cGxvYWRzXC8yMDIxXC8xMFwvYW5hbGl6YS10ZXJtaWNhLTUucG5nIiwic2xpZGVzaG93IjoiMjgyYjhjNyJ9\">\n\t\t\t\t\t<div class=\"e-gallery-image elementor-gallery-item__image\" data-thumbnail=\"https:\/\/foodsafety.upb.ro\/wp-content\/uploads\/2021\/10\/analiza-termica-5.png\" data-width=\"643\" data-height=\"475\" aria-label=\"\" role=\"img\" ><\/div>\n\t\t\t\t\t\t\t\t\t\t\t<div class=\"elementor-gallery-item__overlay\"><\/div>\n\t\t\t\t\t\t\t\t\t\t\t\t\t\t<\/a>\n\t\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t<section class=\"elementor-section elementor-top-section elementor-element elementor-element-9611b2d elementor-section-boxed elementor-section-height-default elementor-section-height-default\" data-id=\"9611b2d\" data-element_type=\"section\" data-e-type=\"section\">\n\t\t\t\t\t\t\t<div class=\"elementor-background-overlay\"><\/div>\n\t\t\t\t\t\t\t<div class=\"elementor-container elementor-column-gap-default\">\n\t\t\t\t\t<div class=\"elementor-column elementor-col-100 elementor-top-column elementor-element elementor-element-4972df9\" data-id=\"4972df9\" data-element_type=\"column\" data-e-type=\"column\">\n\t\t\t<div class=\"elementor-widget-wrap elementor-element-populated\">\n\t\t\t\t\t\t<div class=\"elementor-element elementor-element-ade84d0 elementor-widget elementor-widget-menu-anchor\" data-id=\"ade84d0\" data-element_type=\"widget\" data-e-type=\"widget\" data-widget_type=\"menu-anchor.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t<div class=\"elementor-menu-anchor\" id=\"echipamentdeanaliza\"><\/div>\n\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<div class=\"elementor-element elementor-element-99ba688 elementor-widget elementor-widget-heading\" data-id=\"99ba688\" data-element_type=\"widget\" data-e-type=\"widget\" data-widget_type=\"heading.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t<h2 class=\"elementor-heading-title elementor-size-default\">Echipament de analiz\u0103 elemental\u0103 CHNOS<\/h2>\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<div class=\"elementor-element elementor-element-51f56d0 elementor-widget elementor-widget-spacer\" data-id=\"51f56d0\" data-element_type=\"widget\" data-e-type=\"widget\" data-widget_type=\"spacer.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t<div class=\"elementor-spacer\">\n\t\t\t<div class=\"elementor-spacer-inner\"><\/div>\n\t\t<\/div>\n\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<section class=\"elementor-section elementor-inner-section elementor-element elementor-element-5b2abb2 elementor-section-boxed elementor-section-height-default elementor-section-height-default\" data-id=\"5b2abb2\" data-element_type=\"section\" data-e-type=\"section\">\n\t\t\t\t\t\t<div class=\"elementor-container elementor-column-gap-no\">\n\t\t\t\t\t<div class=\"elementor-column elementor-col-50 elementor-inner-column elementor-element elementor-element-c3763b9\" data-id=\"c3763b9\" data-element_type=\"column\" data-e-type=\"column\">\n\t\t\t<div class=\"elementor-widget-wrap elementor-element-populated\">\n\t\t\t\t\t\t<div class=\"elementor-element elementor-element-3a88134 elementor-widget elementor-widget-text-editor\" data-id=\"3a88134\" data-element_type=\"widget\" data-e-type=\"widget\" data-widget_type=\"text-editor.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t\t\t<p><span style=\"font-weight: 400;\">Cunoa\u0219terea compozi\u021biei elementelor organice \u00eei ajut\u0103 \u0219i pe anali\u0219ti s\u0103 determine structura substan\u021bei e\u0219antionului. Caracterizarea chimic\u0103 a compu\u0219ilor organici este utilizat\u0103 \u00een cercetare, precum \u0219i pentru controlul calit\u0103\u021bii. Este o tehnic\u0103 fiabil\u0103 \u0219i rentabil\u0103 utilizat\u0103 pentru a evalua puritatea \u0219i compozi\u021bia chimic\u0103 a compu\u0219ilor \u0219i poate fi utilizat\u0103 pe o gam\u0103 larg\u0103 de probe.\u00a0<\/span><\/p><p><span style=\"font-weight: 400;\">Cea mai comun\u0103 tehnic\u0103 de analiz\u0103 elemental\u0103 CHNS-O se bazeaz\u0103 pe arderea e\u0219antionului. La ardere, proba genereaz\u0103 gaze compuse ale elementelor C, H, N \u0219i S. Ace\u0219ti produ\u0219i de ardere (de exemplu CO<\/span><span style=\"font-weight: 400;\">2<\/span><span style=\"font-weight: 400;\">, H<\/span><span style=\"font-weight: 400;\">2<\/span><span style=\"font-weight: 400;\">O, NO<\/span><span style=\"font-weight: 400;\">2<\/span><span style=\"font-weight: 400;\"> etc.) sunt m\u0103sura\u021bi utiliz\u00e2nd cromatografia gazoas\u0103 \u0219i, astfel, raportul elementelor din proba original\u0103 este determinat. Elementele C, H, N \u0219i S pot fi analizate simultan, \u00een timp ce O poate fi analizat \u00eentr-o a doua etap\u0103 prin piroliz\u0103. Deoarece cantit\u0103\u021bile finale ale fiec\u0103rui element sunt de obicei date ca procent din greutatea e\u0219antionului original, este esen\u021bial ca e\u0219antionul s\u0103 fie c\u00e2nt\u0103rit cu precizie. Datorit\u0103 dimensiunii foarte mici a e\u0219antionului, se recomand\u0103 o microbalan\u021b\u0103 foarte precis\u0103.<\/span><\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t<div class=\"elementor-column elementor-col-50 elementor-inner-column elementor-element elementor-element-d388809\" data-id=\"d388809\" data-element_type=\"column\" data-e-type=\"column\" data-settings=\"{&quot;background_background&quot;:&quot;classic&quot;}\">\n\t\t\t<div class=\"elementor-widget-wrap elementor-element-populated\">\n\t\t\t\t\t\t<div class=\"elementor-element elementor-element-8a8bf1f elementor-widget elementor-widget-spacer\" data-id=\"8a8bf1f\" data-element_type=\"widget\" data-e-type=\"widget\" data-widget_type=\"spacer.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t<div class=\"elementor-spacer\">\n\t\t\t<div class=\"elementor-spacer-inner\"><\/div>\n\t\t<\/div>\n\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t<div class=\"elementor-element elementor-element-38a43c1 elementor-widget elementor-widget-text-editor\" data-id=\"38a43c1\" data-element_type=\"widget\" data-e-type=\"widget\" data-widget_type=\"text-editor.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t\t\t<p><span style=\"font-weight: 400;\">Analizorul elemental FLASH 2000 (Thermo Scientific\u2122) este echipat cu:<\/span><\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<div class=\"elementor-element elementor-element-f12dc31 elementor-icon-list--layout-traditional elementor-list-item-link-full_width elementor-widget elementor-widget-icon-list\" data-id=\"f12dc31\" data-element_type=\"widget\" data-e-type=\"widget\" data-widget_type=\"icon-list.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t<ul class=\"elementor-icon-list-items\">\n\t\t\t\t\t\t\t<li class=\"elementor-icon-list-item\">\n\t\t\t\t\t\t\t\t\t\t\t<span class=\"elementor-icon-list-icon\">\n\t\t\t\t\t\t\t<i aria-hidden=\"true\" class=\"icon icon-arrow-right\"><\/i>\t\t\t\t\t\t<\/span>\n\t\t\t\t\t\t\t\t\t\t<span class=\"elementor-icon-list-text\">2 reactoare<\/span>\n\t\t\t\t\t\t\t\t\t<\/li>\n\t\t\t\t\t\t\t\t<li class=\"elementor-icon-list-item\">\n\t\t\t\t\t\t\t\t\t\t\t<span class=\"elementor-icon-list-icon\">\n\t\t\t\t\t\t\t<i aria-hidden=\"true\" class=\"icon icon-arrow-right\"><\/i>\t\t\t\t\t\t<\/span>\n\t\t\t\t\t\t\t\t\t\t<span class=\"elementor-icon-list-text\">Detector de conductivitate termic\u0103 (TCD) <\/span>\n\t\t\t\t\t\t\t\t\t<\/li>\n\t\t\t\t\t\t\t\t<li class=\"elementor-icon-list-item\">\n\t\t\t\t\t\t\t\t\t\t\t<span class=\"elementor-icon-list-icon\">\n\t\t\t\t\t\t\t<i aria-hidden=\"true\" class=\"icon icon-arrow-right\"><\/i>\t\t\t\t\t\t<\/span>\n\t\t\t\t\t\t\t\t\t\t<span class=\"elementor-icon-list-text\">Coloan\u0103 analitic\u0103 cromatografic\u0103 - efectueaz\u0103 separarea cromatografic\u0103 a produ\u0219ilor de reac\u021bie genera\u021bi \u00een timpul procesului de ardere sau piroliz\u0103.<\/span>\n\t\t\t\t\t\t\t\t\t<\/li>\n\t\t\t\t\t\t\t\t<li class=\"elementor-icon-list-item\">\n\t\t\t\t\t\t\t\t\t\t\t<span class=\"elementor-icon-list-icon\">\n\t\t\t\t\t\t\t<i aria-hidden=\"true\" class=\"icon icon-arrow-right\"><\/i>\t\t\t\t\t\t<\/span>\n\t\t\t\t\t\t\t\t\t\t<span class=\"elementor-icon-list-text\">Ultramicrobalan\u021b\u0103 Mettler Toledo XP6<\/span>\n\t\t\t\t\t\t\t\t\t<\/li>\n\t\t\t\t\t\t<\/ul>\n\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<div class=\"elementor-element elementor-element-8b42630 elementor-widget elementor-widget-text-editor\" data-id=\"8b42630\" data-element_type=\"widget\" data-e-type=\"widget\" data-widget_type=\"text-editor.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t\t\t<p><span style=\"font-weight: 400;\">Instrumentul este complet controlat de calculator prin intermediul software-ului dedicat, Eager Xperience, utilizat at\u00e2t pentru achizi\u021bie, c\u00e2t \u0219i pentru prelucrarea \u0219i interpretarea rezultatelor ob\u021binute.<\/span><\/p><p><span style=\"font-weight: 400;\">Analizorul elemental, poate fi folosit pentru determinarea concentra\u021biilor de sulf, oxigen, azot, hidrogen \u0219i carbon din probe solide, precum cele alimentare sau probe biologice.<\/span><\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<div class=\"elementor-element elementor-element-1d95e08 elementor-widget elementor-widget-gallery\" data-id=\"1d95e08\" data-element_type=\"widget\" data-e-type=\"widget\" data-settings=\"{&quot;columns_mobile&quot;:2,&quot;lazyload&quot;:&quot;yes&quot;,&quot;gallery_layout&quot;:&quot;grid&quot;,&quot;columns&quot;:4,&quot;columns_tablet&quot;:2,&quot;gap&quot;:{&quot;unit&quot;:&quot;px&quot;,&quot;size&quot;:10,&quot;sizes&quot;:[]},&quot;gap_tablet&quot;:{&quot;unit&quot;:&quot;px&quot;,&quot;size&quot;:10,&quot;sizes&quot;:[]},&quot;gap_mobile&quot;:{&quot;unit&quot;:&quot;px&quot;,&quot;size&quot;:10,&quot;sizes&quot;:[]},&quot;link_to&quot;:&quot;file&quot;,&quot;aspect_ratio&quot;:&quot;3:2&quot;,&quot;overlay_background&quot;:&quot;yes&quot;,&quot;content_hover_animation&quot;:&quot;fade-in&quot;}\" data-widget_type=\"gallery.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t<div class=\"elementor-gallery__container\">\n\t\t\t\t\t\t\t<a class=\"e-gallery-item elementor-gallery-item elementor-animated-content\" href=\"https:\/\/foodsafety.upb.ro\/wp-content\/uploads\/2021\/10\/analiza-elementala-3.png\" data-elementor-open-lightbox=\"yes\" data-elementor-lightbox-slideshow=\"1d95e08\" data-elementor-lightbox-title=\"analiza elementala 3\" data-e-action-hash=\"#elementor-action%3Aaction%3Dlightbox%26settings%3DeyJpZCI6MTM5MSwidXJsIjoiaHR0cHM6XC9cL2Zvb2RzYWZldHkudXBiLnJvXC93cC1jb250ZW50XC91cGxvYWRzXC8yMDIxXC8xMFwvYW5hbGl6YS1lbGVtZW50YWxhLTMucG5nIiwic2xpZGVzaG93IjoiMWQ5NWUwOCJ9\">\n\t\t\t\t\t<div class=\"e-gallery-image elementor-gallery-item__image\" data-thumbnail=\"https:\/\/foodsafety.upb.ro\/wp-content\/uploads\/2021\/10\/analiza-elementala-3.png\" data-width=\"423\" data-height=\"255\" aria-label=\"\" role=\"img\" ><\/div>\n\t\t\t\t\t\t\t\t\t\t\t<div class=\"elementor-gallery-item__overlay\"><\/div>\n\t\t\t\t\t\t\t\t\t\t\t\t\t\t<\/a>\n\t\t\t\t\t\t\t<a class=\"e-gallery-item elementor-gallery-item elementor-animated-content\" href=\"https:\/\/foodsafety.upb.ro\/wp-content\/uploads\/2021\/10\/analiza-elementala-2.png\" data-elementor-open-lightbox=\"yes\" data-elementor-lightbox-slideshow=\"1d95e08\" data-elementor-lightbox-title=\"analiza elementala 2\" data-e-action-hash=\"#elementor-action%3Aaction%3Dlightbox%26settings%3DeyJpZCI6MTM5MiwidXJsIjoiaHR0cHM6XC9cL2Zvb2RzYWZldHkudXBiLnJvXC93cC1jb250ZW50XC91cGxvYWRzXC8yMDIxXC8xMFwvYW5hbGl6YS1lbGVtZW50YWxhLTIucG5nIiwic2xpZGVzaG93IjoiMWQ5NWUwOCJ9\">\n\t\t\t\t\t<div class=\"e-gallery-image elementor-gallery-item__image\" data-thumbnail=\"https:\/\/foodsafety.upb.ro\/wp-content\/uploads\/2021\/10\/analiza-elementala-2.png\" data-width=\"332\" data-height=\"169\" aria-label=\"\" role=\"img\" ><\/div>\n\t\t\t\t\t\t\t\t\t\t\t<div class=\"elementor-gallery-item__overlay\"><\/div>\n\t\t\t\t\t\t\t\t\t\t\t\t\t\t<\/a>\n\t\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t<\/div>\n\t\t","protected":false},"excerpt":{"rendered":"<p>Laboratorul de analiz\u0103 termic\u0103 complex\u0103 Aparat de analiz\u0103 complex\u0103 (ATD-DSC-TG-FTIR-MS) Echipament de analiz\u0103 elemental\u0103 CHNOS Aparat de analiz\u0103 complex\u0103 (ATD-DSC-TG-FTIR-MS) Sistemul de analiz\u0103 termic\u0103 complex\u0103 format dintr-o termobalan\u0163\u0103 STA 449 C F3 de la Netzsch, care poate analiza pierderile de mas\u0103 \u00een intervalul -100 \u2013 1000oC (prin r\u0103cire cu azot lichid). Viteza de \u00eenc\u0103lzire a [&hellip;]<\/p>\n","protected":false},"author":2,"featured_media":0,"parent":0,"menu_order":0,"comment_status":"closed","ping_status":"closed","template":"elementor_header_footer","meta":{"footnotes":""},"class_list":["post-501","page","type-page","status-publish","hentry"],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v27.4 - https:\/\/yoast.com\/product\/yoast-seo-wordpress\/ -->\n<title>Laboratorul de analiz\u0103 termic\u0103 complex\u0103 - FoodSafety<\/title>\n<meta name=\"description\" content=\"Cunoa\u0219terea compozi\u021biei elementelor organice \u00eei ajut\u0103 \u0219i pe anali\u0219ti s\u0103 determine structura substan\u021bei e\u0219antionului.\" \/>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/foodsafety.upb.ro\/en\/laboratorul-de-analiza-termica-complexa\/\" \/>\n<meta property=\"og:locale\" content=\"en_US\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"Laboratorul de analiz\u0103 termic\u0103 complex\u0103 - 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