Exploitation of the magnetic nanoparticles in developing magnetic microdevice

Coordinator - Polytechnic University of Bucharest 

Project leader: Professor Ecaterina ANDRONESCU

Research member: Professor Paul SVASTA

Research member: Professor Anton FICAI

Research member: Professor Ciprian IONESCU

Research member: Associate professor Denisa FICAI

Research member: Professor Norocel Dragos CODREANU

Research member: Scientific Research III Bogdan Ștefan VASILE

Lector Universitar: Lector Mihaela PANTAZICĂ

Lector Universitar: Lector Bogdan MIHĂILESCU

Research member: Scientific Research Assistant Angela SPOIALĂ

Research member: University Assistant Adrian Vasile SURDU

Research member: Scientific Research Assistant Georgiana DOLETE

Research member: Scientific Research Assistant Alexa Maria CROITORU

Research member: Scientific Research Assistant Alexandra Cătălina BÎRCĂ

Research member: Technician eng. Teodor MIHĂILESCUc

Research member: Technician eng. Delia Georgeta LEPĂDATU

Partener (P1) – NANOM MEMS SRL

Person in charge PhD eng. Marin GHEORGHE

Research member: Scientific Researcher Simona GHEORGHE

PROJECT SCOPE 

The project involves the development of an experimental model of electromagnetically actuated micropumps for applications in the field of microfluidics. The work plan proposed in this project is focused on the formulation of magnetic pastes / inks for screen-printing technology, so that these separate components could be integrated in the fabrication of micropumps for further exploitations in BioMEMS devices. Literature in the field presents various methods for actuating micropumps, among which electromagnetic actuation has a number of significant advantages such as superior response time and most importantly the lack of interactions with (bio) chemical or biological fluids. Research activities are carried out in effective collaboration between University POLITEHNICA of Bucharest and NANOM MEMS SRL and involves preliminary studies to obtain magnetic nanoparticles; formulation of magnetic pastes/inks with predetermined characteristics; initiation of magnetic pastes/inks depositions on specific substrates used in BioMEMS devices, followed by complex characterizations regarding physico-chemical properties, including electrical ones. Also, the functionality of the developed films will be tested at laboratory level to prove their actuation characteristics. To optimize the performances of the formulations of magnetic inks/pastes, special attention will be paid to the development of magnetic nanoparticles with desired size, but also functionalized according to the polymeric component of the paste. The commitment of our partner (NANOM MEMS SRL) is very important for the project, the company being interested in future transposition of the research on market. Given these circumstances, the project assumes additional stability tests, including dynamic tests with simulated flowing liquids, especially considering biological applications.

The project aims to develop intelligent materials for the magnetic actuation of BioMEMS devices. More precisely, the project proposes the development of magnetic pastes/inks with physico-chemical and mechanical properties specific to deposition technologies, in order to obtain an integrated demonstration model of electromagnetically operated micropump with applicability in BioMEMS devices (microelectromechanical systems with biological applications).

 

  • Co-precipitation of Fe3+ and Me2+ (Me = Fe, Co, Ni, ...) to generate easily dispersible magnetic fluids / pastes
  • Starting the stage of optimization of the synthesis conditions to obtain dispersible nanoparticles with reduced agglomeration tendency, selection of suitable stabilizing agents, identification of multifunctional agents with stabilization potential and binding to polymeric resin
  • Optimization of the synthesis conditions in order to obtain dispersible nanoparticles with reduced agglomeration tendency, selection of suitable stabilizing agents, identification of multifunctional agents with stabilization potential and binding to polymeric resin.
  • Selection of polymer(s) to be used as binder(s) for ferromagnetic powders.
  • Compositional, morpho-structural and dimensional evaluation of magnetic nanopowders, evaluation of colloidal and chemical stability using modern techniques: FTIR, XRD, VSM, SEM, TEM, ATD-TG, DLS etc.
  • Chemical modification of the surface of magnetic nanoparticles to assure compatibility with the polymers used as a binder.
  • Industrial research regarding testing of the magnetic pastes with characteristics adapted to various deposition technologies (screen printing, dr. Blade, dip coating etc.).
  • Characterization of the films deposited (FTIR, XRD, SEM, TEM, ATD-TG etc.):
    Evaluation of the stability of magnetic pastes / inks (segregation, oxidation etc.) but also of the adhesion of the deposits and its continuity; assessment of electrical properties of deposits
  • Evaluation of the stability of magnetic pastes / inks (segregation, oxidation etc.) but also of the adhesion of the deposits and its continuity; assessment of electrical properties of deposits
  • Selection of the optimum experimental models of the masks to be used for the deposition of the functional layers.
  • Design of the proper geometric models for the development of micro-pumps and magnetic actuators.
  • Testing the obtained deposits in the context of magnetic actuator devices.
  • Industrial research regarding optimal deposition techniques for obtaining magnetically actuated devices.
  • Assessment of the functionality of magnetic films
  • Evaluation of stability of deposits under simulated conditions (including in humid environments)
  • Optimization of the films in order to enhance the functional parameters magneto-electric properties
  • Functionality testing of the devices